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Complex material and surface analysis of anterolateral distal tibial plate of 1.4441 steel

Identifikátory výsledku

  • Kód výsledku v IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00843989%3A_____%2F22%3AE0109448" target="_blank" >RIV/00843989:_____/22:E0109448 - isvavai.cz</a>

  • Nalezeny alternativní kódy

    RIV/61989100:27230/21:10249114 RIV/61989100:27360/21:10249114 RIV/61989100:27690/21:10249114 RIV/61988987:17110/22:A2302FLU

  • Výsledek na webu

    <a href="https://www.mdpi.com/2075-4701/12/1/60" target="_blank" >https://www.mdpi.com/2075-4701/12/1/60</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.3390/met12010060" target="_blank" >10.3390/met12010060</a>

Alternativní jazyky

  • Jazyk výsledku

    angličtina

  • Název v původním jazyce

    Complex material and surface analysis of anterolateral distal tibial plate of 1.4441 steel

  • Popis výsledku v původním jazyce

    Nickel-based austenitic stainless steels are still common for manufacture of implants intended for acute hard tissue reinforcement or stabilization, but the risk of negative reactions due to soluble nickel-rich corrosion products must be considered seriously. Corrosion processes may even be accelerated by the evolution of microstructure caused by excessive heat during machining, etc. Therefore, this study also deals with the investigation of microstructure and microhardness changes near the threaded holes of the anterolateral distal tibial plate containing approx. 14wt.% Ni by composition. There were only insignificant changes of microhardness, grain size, or microstructure orientation found close to the area of machining. In addition, wettability measurements of surface energy demonstrated only minor differences for bulk material and areas close to machining. The cyclic potentiodynamic polarization tests were performed in isotonic physiological solution. The first cycle was used for the determination of corrosion characteristics of the implant after chemical passivation, the second cycle was used to simulate real material behavior under the condition of previous surface damage by excessive pitting corrosion occurring during previous polarization. It was found that the damaged and spontaneously repassived surface showed a three-time higher standard corrosion rate than the “as received” chemically passivated surface. One may conclude that previous surface damage may decrease the lifetime of the implant significantly and increase the amount of nickel-based corrosion products distributed into surrounding tissues.

  • Název v anglickém jazyce

    Complex material and surface analysis of anterolateral distal tibial plate of 1.4441 steel

  • Popis výsledku anglicky

    Nickel-based austenitic stainless steels are still common for manufacture of implants intended for acute hard tissue reinforcement or stabilization, but the risk of negative reactions due to soluble nickel-rich corrosion products must be considered seriously. Corrosion processes may even be accelerated by the evolution of microstructure caused by excessive heat during machining, etc. Therefore, this study also deals with the investigation of microstructure and microhardness changes near the threaded holes of the anterolateral distal tibial plate containing approx. 14wt.% Ni by composition. There were only insignificant changes of microhardness, grain size, or microstructure orientation found close to the area of machining. In addition, wettability measurements of surface energy demonstrated only minor differences for bulk material and areas close to machining. The cyclic potentiodynamic polarization tests were performed in isotonic physiological solution. The first cycle was used for the determination of corrosion characteristics of the implant after chemical passivation, the second cycle was used to simulate real material behavior under the condition of previous surface damage by excessive pitting corrosion occurring during previous polarization. It was found that the damaged and spontaneously repassived surface showed a three-time higher standard corrosion rate than the “as received” chemically passivated surface. One may conclude that previous surface damage may decrease the lifetime of the implant significantly and increase the amount of nickel-based corrosion products distributed into surrounding tissues.

Klasifikace

  • Druh

    J<sub>imp</sub> - Článek v periodiku v databázi Web of Science

  • CEP obor

  • OECD FORD obor

    30404 - Biomaterials (as related to medical implants, devices, sensors)

Návaznosti výsledku

  • Projekt

    <a href="/cs/project/EF17_049%2F0008441" target="_blank" >EF17_049/0008441: Inovativní léčebné metody pohybového aparátu v úrazové chirurgii</a><br>

  • Návaznosti

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Ostatní

  • Rok uplatnění

    2022

  • Kód důvěrnosti údajů

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Údaje specifické pro druh výsledku

  • Název periodika

    Metals

  • ISSN

    2075-4701

  • e-ISSN

  • Svazek periodika

    12

  • Číslo periodika v rámci svazku

    article 60

  • Stát vydavatele periodika

    CH - Švýcarská konfederace

  • Počet stran výsledku

    14

  • Strana od-do

    1-14

  • Kód UT WoS článku

    000747770300001

  • EID výsledku v databázi Scopus

    2-s2.0-85121754066