Synthesis and crystal structure of [Pb(gly)2]n New lead(II) coordination polymer with glycine ligand

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F19%3A00519691" target="_blank" >RIV/68378271:_____/19:00519691 - isvavai.cz</a>

Výsledek na webu

<a href="https://doi.org/10.22052/JNS.2019.01.02" target="_blank" >https://doi.org/10.22052/JNS.2019.01.02</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.22052/JNS.2019.01.02" target="_blank" >10.22052/JNS.2019.01.02</a>

Jazyk výsledku

angličtina

Název v původním jazyce

Synthesis and crystal structure of [Pb(gly)2]n New lead(II) coordination polymer with glycine ligand

Popis výsledku v původním jazyce

The [Pb(gly)2]n (1) have been synthesized and characterized by elemental analyses, IR, 1H NMR and 13C NMR spectroscopy. The single crystal structure of 1 show the complex is 2D coordination polymer with octahedral environment that is formed into 3D supramolecule through hydrogen bond. Structural determination of compound 1 reveals the Pb(II) ion is four coordinated, bonded to a nitrogen, oxygen and two carbon atoms from the Glycine ligand. PbO nanoparticles were synthesized by calcinations of compound 1 at 500, 550 and 600 °C under air atmosphere. The PbO nanostructure was characterized by scanning electron microscopy and X-ray powder diffraction. The thermal stability of compound 1 was studied by thermal gravimetric and differential thermal analyses.

Název v anglickém jazyce

Synthesis and crystal structure of [Pb(gly)2]n New lead(II) coordination polymer with glycine ligand

Popis výsledku anglicky

The [Pb(gly)2]n (1) have been synthesized and characterized by elemental analyses, IR, 1H NMR and 13C NMR spectroscopy. The single crystal structure of 1 show the complex is 2D coordination polymer with octahedral environment that is formed into 3D supramolecule through hydrogen bond. Structural determination of compound 1 reveals the Pb(II) ion is four coordinated, bonded to a nitrogen, oxygen and two carbon atoms from the Glycine ligand. PbO nanoparticles were synthesized by calcinations of compound 1 at 500, 550 and 600 °C under air atmosphere. The PbO nanostructure was characterized by scanning electron microscopy and X-ray powder diffraction. The thermal stability of compound 1 was studied by thermal gravimetric and differential thermal analyses.

Druh

J_imp - Článek v periodiku v databázi Web of Science

CEP obor

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OECD FORD obor

10302 - Condensed matter physics (including formerly solid state physics, supercond.)

Projekt

—

Návaznosti

I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Rok uplatnění

2019

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název periodika

JOURNAL OF NANOSTRUCTURES

ISSN

2251-7871

e-ISSN

—

Svazek periodika

9

Číslo periodika v rámci svazku

1

Stát vydavatele periodika

IR - Íránská islámská republika

Počet stran výsledku

6

Strana od-do

8-13

Kód UT WoS článku

000468626700002

EID výsledku v databázi Scopus

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