Synthesis and characterization of new coordination polymer with l-proline amino acid ligand, new precursor for preparation of pure phase lead(II) oxide nanoparticles via thermal decomposition

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F17%3A00482858" target="_blank" >RIV/68378271:_____/17:00482858 - isvavai.cz</a>

Výsledek na webu

<a href="http://dx.doi.org/10.1007/s13738-017-1162-5" target="_blank" >http://dx.doi.org/10.1007/s13738-017-1162-5</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1007/s13738-017-1162-5" target="_blank" >10.1007/s13738-017-1162-5</a>

Jazyk výsledku

angličtina

Název v původním jazyce

Synthesis and characterization of new coordination polymer with l-proline amino acid ligand, new precursor for preparation of pure phase lead(II) oxide nanoparticles via thermal decomposition

Popis výsledku v původním jazyce

A new two-dimensional lead(II) coordination polymer, [Pb(Pro)2]n (1), Pro = l-proline amino acid, has been synthesized and characterized by IR and X-ray diffraction. Structural determination reveals the Pb(II) ion is four-coordinated, bonded to two nitrogen atoms and two oxygen atoms from the l-proline ligand. PbO nanoparticles were synthesized by calcination at 500, 550 and 600 °C under air atmosphere. The PbO nanostructure was characterized by scanning electron microscopy (SEM) and X-ray powder diffraction (XRD). The thermal stability was studied by thermal gravimetric analysis (TGA) and diffe rential thermal analysis (DTA).n

Název v anglickém jazyce

Synthesis and characterization of new coordination polymer with l-proline amino acid ligand, new precursor for preparation of pure phase lead(II) oxide nanoparticles via thermal decomposition

Popis výsledku anglicky

A new two-dimensional lead(II) coordination polymer, [Pb(Pro)2]n (1), Pro = l-proline amino acid, has been synthesized and characterized by IR and X-ray diffraction. Structural determination reveals the Pb(II) ion is four-coordinated, bonded to two nitrogen atoms and two oxygen atoms from the l-proline ligand. PbO nanoparticles were synthesized by calcination at 500, 550 and 600 °C under air atmosphere. The PbO nanostructure was characterized by scanning electron microscopy (SEM) and X-ray powder diffraction (XRD). The thermal stability was studied by thermal gravimetric analysis (TGA) and diffe rential thermal analysis (DTA).n

Druh

J_imp - Článek v periodiku v databázi Web of Science

CEP obor

—

OECD FORD obor

10302 - Condensed matter physics (including formerly solid state physics, supercond.)

Projekt

—

Návaznosti

I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Rok uplatnění

2017

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název periodika

Journal of the Iranian Chemical Society

ISSN

1735-207X

e-ISSN

—

Svazek periodika

14

Číslo periodika v rámci svazku

11

Stát vydavatele periodika

IR - Íránská islámská republika

Počet stran výsledku

7

Strana od-do

2255-2261

Kód UT WoS článku

000413262100001

EID výsledku v databázi Scopus

2-s2.0-85032008857