Fast HPLC Method for Determination of Fenoxycarb and Permethrin in Antiparasitic Veterinary Shampoo Using Fused-Core Column

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11160%2F13%3A10146040" target="_blank" >RIV/00216208:11160/13:10146040 - isvavai.cz</a>

Výsledek na webu

<a href="http://link.springer.com/article/10.1007/s10337-013-2464-0/fulltext.html" target="_blank" >http://link.springer.com/article/10.1007/s10337-013-2464-0/fulltext.html</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1007/s10337-013-2464-0" target="_blank" >10.1007/s10337-013-2464-0</a>

Jazyk výsledku

angličtina

Název v původním jazyce

Fast HPLC Method for Determination of Fenoxycarb and Permethrin in Antiparasitic Veterinary Shampoo Using Fused-Core Column

Popis výsledku v původním jazyce

A new and fast high-performance liquid chromatography (HPLC) method using technology of fused-core columns for separation of fenoxycarb and cis-, trans-permethrin has been developed and used for their determination in antiparasitic veterinary shampoo. Separation of insecticides and internal standard sudan II was achieved on the fused-core column Ascentis Express RP-Amide (100 x 3.0 mm), particle size 2.7 mu m, with mobile phase acetonitrile/water (55:45, v/v) at a flow rate of 1.0 mL min(-1) and at temperature 60 A degrees C. The detection wavelength of detector was set at 225 nm for both compounds and internal standard sudan II. Under the optimum chromatographic conditions standard calibration curves were measured with good linearity [r (2) = 0.99991for fenoxycarb, r (2) = 0.99987 for trans-permethrin, and r (2) = 0.99984 for cis-permethrin (n = 8)]. Commercial samples of antiparasitic veterinary shampoo were extracted with ethanol in ultrasound bath for 5 min. A 2-mu L sample volume

Název v anglickém jazyce

Fast HPLC Method for Determination of Fenoxycarb and Permethrin in Antiparasitic Veterinary Shampoo Using Fused-Core Column

Popis výsledku anglicky

A new and fast high-performance liquid chromatography (HPLC) method using technology of fused-core columns for separation of fenoxycarb and cis-, trans-permethrin has been developed and used for their determination in antiparasitic veterinary shampoo. Separation of insecticides and internal standard sudan II was achieved on the fused-core column Ascentis Express RP-Amide (100 x 3.0 mm), particle size 2.7 mu m, with mobile phase acetonitrile/water (55:45, v/v) at a flow rate of 1.0 mL min(-1) and at temperature 60 A degrees C. The detection wavelength of detector was set at 225 nm for both compounds and internal standard sudan II. Under the optimum chromatographic conditions standard calibration curves were measured with good linearity [r (2) = 0.99991for fenoxycarb, r (2) = 0.99987 for trans-permethrin, and r (2) = 0.99984 for cis-permethrin (n = 8)]. Commercial samples of antiparasitic veterinary shampoo were extracted with ethanol in ultrasound bath for 5 min. A 2-mu L sample volume

Druh

J_x - Nezařazeno - Článek v odborném periodiku (Jimp, Jsc a Jost)

CEP obor

CB - Analytická chemie, separace

OECD FORD obor

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Projekt

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Návaznosti

I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Rok uplatnění

2013

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název periodika

Chromatographia

ISSN

0009-5893

e-ISSN

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Svazek periodika

76

Číslo periodika v rámci svazku

21-22

Stát vydavatele periodika

NL - Nizozemsko

Počet stran výsledku

6

Strana od-do

1559-1564

Kód UT WoS článku

000326118900018

EID výsledku v databázi Scopus

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