Effects of etchant stirring on the surface quality of the metallography sample

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68081731%3A_____%2F23%3A00575706" target="_blank" >RIV/68081731:_____/23:00575706 - isvavai.cz</a>

Výsledek na webu

<a href="https://iopscience.iop.org/article/10.1088/1742-6596/2572/1/012011" target="_blank" >https://iopscience.iop.org/article/10.1088/1742-6596/2572/1/012011</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1088/1742-6596/2572/1/012011" target="_blank" >10.1088/1742-6596/2572/1/012011</a>

Jazyk výsledku

angličtina

Název v původním jazyce

Effects of etchant stirring on the surface quality of the metallography sample

Popis výsledku v původním jazyce

Despite its predominantly empirical nature, metallographic etching remains an important sample preparation method that enables microstructural characterization. The poor repeatability is due to the ignorance of etching mechanisms and the human factor, which is mainly associated with the conventional approach. This approach is most commonly practiced by manual immersion of the sample in the etchant. The solution should be gently stirred so that reaction products do not settle on the surface and uneven etching does not occur. Often, stirring is provided by the sample itself or by a magnetic bar. In terms of spatial orientation, etching with the polished surface facing upwards allows the surface to be observed during the process. Some authors recommend etching with the polished surface downwards to minimize the deposition of reaction products. In some cases, a vertical orientation of the sample is recommended to reduce pitting. In this paper, the effect of the etchant stirring method on the surface quality of a metallographic structural steel specimen will be presented. In addition to different etchant stirring methods, different spatial orientations of the sample will also be investigated. To ensure better repeatability and accurate etching time, the samples will be etched using our automated apparatus. The resulting surface of the samples will be analysed using light optical microscopy (LOM) and confocal laser scanning microscopy (CLSM). The development of more reproducible etching methods is essential to obtain accurate microstructure information without artifacts and for advanced quantitative image analysis using deep learning.

Název v anglickém jazyce

Effects of etchant stirring on the surface quality of the metallography sample

Popis výsledku anglicky

Despite its predominantly empirical nature, metallographic etching remains an important sample preparation method that enables microstructural characterization. The poor repeatability is due to the ignorance of etching mechanisms and the human factor, which is mainly associated with the conventional approach. This approach is most commonly practiced by manual immersion of the sample in the etchant. The solution should be gently stirred so that reaction products do not settle on the surface and uneven etching does not occur. Often, stirring is provided by the sample itself or by a magnetic bar. In terms of spatial orientation, etching with the polished surface facing upwards allows the surface to be observed during the process. Some authors recommend etching with the polished surface downwards to minimize the deposition of reaction products. In some cases, a vertical orientation of the sample is recommended to reduce pitting. In this paper, the effect of the etchant stirring method on the surface quality of a metallographic structural steel specimen will be presented. In addition to different etchant stirring methods, different spatial orientations of the sample will also be investigated. To ensure better repeatability and accurate etching time, the samples will be etched using our automated apparatus. The resulting surface of the samples will be analysed using light optical microscopy (LOM) and confocal laser scanning microscopy (CLSM). The development of more reproducible etching methods is essential to obtain accurate microstructure information without artifacts and for advanced quantitative image analysis using deep learning.

Druh

D - Stať ve sborníku

CEP obor

—

OECD FORD obor

20501 - Materials engineering

Projekt

<a href="/cs/project/TN01000008" target="_blank" >TN01000008: Centrum elektronové a fotonové optiky</a><br>

Návaznosti

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Rok uplatnění

2023

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název statě ve sborníku

Journal of Physics: Conference Series

ISBN

—

ISSN

1742-6588

e-ISSN

1742-6596

Počet stran výsledku

6

Strana od-do

012011

Název nakladatele

IOP Publishing

Místo vydání

Bristol

Místo konání akce

Pilsen

Datum konání akce

6. 9. 2022

Typ akce podle státní příslušnosti

WRD - Celosvětová akce

Kód UT WoS článku

—