Effects of etchant stirring on the surface quality of the metallography sample
Identifikátory výsledku
Kód výsledku v IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68081731%3A_____%2F23%3A00575706" target="_blank" >RIV/68081731:_____/23:00575706 - isvavai.cz</a>
Výsledek na webu
<a href="https://iopscience.iop.org/article/10.1088/1742-6596/2572/1/012011" target="_blank" >https://iopscience.iop.org/article/10.1088/1742-6596/2572/1/012011</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1088/1742-6596/2572/1/012011" target="_blank" >10.1088/1742-6596/2572/1/012011</a>
Alternativní jazyky
Jazyk výsledku
angličtina
Název v původním jazyce
Effects of etchant stirring on the surface quality of the metallography sample
Popis výsledku v původním jazyce
Despite its predominantly empirical nature, metallographic etching remains an important sample preparation method that enables microstructural characterization. The poor repeatability is due to the ignorance of etching mechanisms and the human factor, which is mainly associated with the conventional approach. This approach is most commonly practiced by manual immersion of the sample in the etchant. The solution should be gently stirred so that reaction products do not settle on the surface and uneven etching does not occur. Often, stirring is provided by the sample itself or by a magnetic bar. In terms of spatial orientation, etching with the polished surface facing upwards allows the surface to be observed during the process. Some authors recommend etching with the polished surface downwards to minimize the deposition of reaction products. In some cases, a vertical orientation of the sample is recommended to reduce pitting. In this paper, the effect of the etchant stirring method on the surface quality of a metallographic structural steel specimen will be presented. In addition to different etchant stirring methods, different spatial orientations of the sample will also be investigated. To ensure better repeatability and accurate etching time, the samples will be etched using our automated apparatus. The resulting surface of the samples will be analysed using light optical microscopy (LOM) and confocal laser scanning microscopy (CLSM). The development of more reproducible etching methods is essential to obtain accurate microstructure information without artifacts and for advanced quantitative image analysis using deep learning.
Název v anglickém jazyce
Effects of etchant stirring on the surface quality of the metallography sample
Popis výsledku anglicky
Despite its predominantly empirical nature, metallographic etching remains an important sample preparation method that enables microstructural characterization. The poor repeatability is due to the ignorance of etching mechanisms and the human factor, which is mainly associated with the conventional approach. This approach is most commonly practiced by manual immersion of the sample in the etchant. The solution should be gently stirred so that reaction products do not settle on the surface and uneven etching does not occur. Often, stirring is provided by the sample itself or by a magnetic bar. In terms of spatial orientation, etching with the polished surface facing upwards allows the surface to be observed during the process. Some authors recommend etching with the polished surface downwards to minimize the deposition of reaction products. In some cases, a vertical orientation of the sample is recommended to reduce pitting. In this paper, the effect of the etchant stirring method on the surface quality of a metallographic structural steel specimen will be presented. In addition to different etchant stirring methods, different spatial orientations of the sample will also be investigated. To ensure better repeatability and accurate etching time, the samples will be etched using our automated apparatus. The resulting surface of the samples will be analysed using light optical microscopy (LOM) and confocal laser scanning microscopy (CLSM). The development of more reproducible etching methods is essential to obtain accurate microstructure information without artifacts and for advanced quantitative image analysis using deep learning.
Klasifikace
Druh
D - Stať ve sborníku
CEP obor
—
OECD FORD obor
20501 - Materials engineering
Návaznosti výsledku
Projekt
<a href="/cs/project/TN01000008" target="_blank" >TN01000008: Centrum elektronové a fotonové optiky</a><br>
Návaznosti
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)
Ostatní
Rok uplatnění
2023
Kód důvěrnosti údajů
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Údaje specifické pro druh výsledku
Název statě ve sborníku
Journal of Physics: Conference Series
ISBN
—
ISSN
1742-6588
e-ISSN
1742-6596
Počet stran výsledku
6
Strana od-do
012011
Název nakladatele
IOP Publishing
Místo vydání
Bristol
Místo konání akce
Pilsen
Datum konání akce
6. 9. 2022
Typ akce podle státní příslušnosti
WRD - Celosvětová akce
Kód UT WoS článku
—